纺织学报 ›› 2015, Vol. 36 ›› Issue (06): 155-161.

• 综合述评 • 上一篇    下一篇

成纤高聚物中无机粒子分散性表征方法及理论研究

  

  • 收稿日期:2014-06-12 修回日期:2014-10-20 出版日期:2015-06-15 发布日期:2015-06-17
  • 通讯作者: 姜兆辉 E-mail:tjjzh_2005@163.com

Study on characterization methods and theories of inorganic particles dispersion in fiber-forming polymers

  • Received:2014-06-12 Revised:2014-10-20 Online:2015-06-15 Published:2015-06-17

摘要:

针对功能性杂化纤维制备过程中微纳米无机粒子分散困难、易于团聚等问题,归纳了传统的无机粒子分散性表征方法,介绍了太赫兹时域光谱、超声波、X-射线相衬成像等新技术。通过综合传统方法和新技术,提出构建以光学显微镜(OM)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)法为主,间接法为辅,并尝试纳入超声法、太赫兹时域光谱及X-射线相衬成像新技术的多级粒径联合评价体系。为深入探究分散性表征方法提供参考。

关键词: 微纳米, 无机粒子, 分散性, 表征方法, 相关理论

Abstract:

In view of difficult dispersion and easy agglomeration of micro-nano inorganic particles in functional hybrid fibers, the traditional characterization methods of inorganic particles dispersion were summarized and new techniques such as terahertz time-domain spectroscopy, ultrasonic wave and X-ray ultramicroscopy were also introduced. The investigation suggests that none of the methods can fully reflect dispersion state of inorganic particles in blending system. In the paper, the multi-level particle size evaluation system was proposed,which is mainly composed by 3M method including OM, SEM and TEM, supplemented by indirect methods. Besides, an attempt of incorporation terahertz time-domain spectroscopy, ultrasonic wave and X-ray ultramicroscopy into the evaluation system was made. To carry on a further reasearch on characterization methods of inorganic particles dispersion, the theories of dispersion characterization were reviewed.

Key words: micro-nano, inorganic particle, dispersion, characterization method, relevant theory

中图分类号: 

  • TQ317.2
[1] 董锋 王航 滕士英 庄旭品 程博闻 . 梯度复合聚丙烯腈纳米纤维膜的制备及其过滤性能[J]. 纺织学报, 2018, 39(09): 1-7.
[2] 袁晓雨 李伟 朱振国 张兴祥. 超疏水聚酯滤布的性能及其在油水分离中的应用[J]. 纺织学报, 2017, 38(03): 108-113.
[3] 辛三法 王新厚 胡守忠. 微纳米纤维的熔喷制作工艺[J]. 纺织学报, 2015, 36(07): 7-0.
[4] 韩春韶;傅雅琴;倪庆清. 溶剂对VGCF/SMPU复合材料形态结构的影响[J]. 纺织学报, 2009, 30(02): 24-28.
[5] 陈晓蕾.;王鲁民.. 纳米ATO在制备抗静电PET单体EG中的分散性[J]. 纺织学报, 2008, 29(6): 1-6.
[6] 张顺花;杨秀琴;杨逢春. 十字形中空纤维异形度的表征方法探讨[J]. 纺织学报, 2008, 29(5): 11-14.
[7] 陈海珍;陈建勇. 纳米氧化钛—乙二醇稳定溶胶体系的制备及在聚酯中的分散性研究[J]. 纺织学报, 2003, 24(01): 30-32.
[8] 毕海峰;张玉梅;王华平;王学利. EM改性聚丙烯纤维的电磁屏蔽性能研究[J]. 纺织学报, 2001, 22(06): 19-20.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
[1] 张朝辉;李梅. 原棉性能与纱线强力的关系[J]. 纺织学报, 2005, 26(1): 52 -53 .
[2] 魏宗升. 小踵趾差盖板的试验分析[J]. 纺织学报, 1987, 8(01): 36 -39 .
[3] 刘亮喜. 永磁式同步电动机的特性和应用中注意的问题[J]. 纺织学报, 1986, 7(05): 47 -50 .
[4] 张林发. 水冲式圆盘回风滤尘器[J]. 纺织学报, 1986, 7(05): 33 .
[5] 黄亚雄;徐步高. 单板机织机产量统计系统[J]. 纺织学报, 1987, 8(11): 42 -44 .
[6] 康阜生;严伟;程远欣;封冰;严迅;巫拱生. 接枝亚麻纤维的工业性试验(三)[J]. 纺织学报, 2004, 25(03): 72 -73 .
[7] 张振义;吴瑜. 气流纺纱新工艺的技术经济分析[J]. 纺织学报, 1984, 5(09): 25 -29 .
[8] 张迎春;蒋秀明;韩旭彤. 德国Malimo缝编机的平行衬纬改造[J]. 纺织学报, 2006, 27(1): 83 -88 .
[9] 纺织品网络辅助设计系统的开发. 纺织品网络辅助设计系统的开发[J]. 纺织学报, 2005, 26(5): 108 -110 .
[10] 李兴弟;杨秀华. 分散染料用苯甲醇/水共沸蒸汽固色的研究[J]. 纺织学报, 1984, 5(08): 11 -15 .