一氯均三嗪-β-环糊精包合驱蚊剂的制备

纺织学报 ›› 2007, Vol. 28 ›› Issue (10): 70-73.

一氯均三嗪-β-环糊精包合驱蚊剂的制备

王树根¹;徐利^2.3

江南大学生态纺织教育部重点实验室江苏无锡214122;西安工程大学陕西西安710048;北京洁尔爽高科技有限公司;上海200082

收稿日期:2006-12-28 修回日期:2007-06-06 出版日期:2007-10-15 发布日期:2007-10-15

Preparation of monochlorotriazinyl-β-cyclodextrin inclusion anti-mosquito complex

WANG Shugen;XU Li

1.Key Laboratory of Science and Technology of Eco-Textile;Ministry of Education;Jiangnan University;Wuxi;Jiangsu 214122;China;2.Xi′an Polytechnic University;Xi′an;Shanxi 710048;China;3.Beijing Jlsun High-Tech Co.;Ltd.;Shanghai 200082;China

Received:2006-12-28 Revised:2007-06-06 Online:2007-10-15 Published:2007-10-15

摘要/Abstract

摘要： 针对一氯均三嗪-β-环糊精(简称MCT--βCD)带有活性基团同时又具有疏水型空腔的特点,研究缓释驱蚊整理剂的制备方法,紫外可见分光光度法证明形成了MCT--βCD与驱蚊剂DEET包合物。MCT--βCD包合驱蚊剂DEET的制备工艺为:主、客体物质的量比为2∶1,温度50℃,时间2 h,搅拌速度300 r/min。包合物耐热耐碱稳定性良好,可以满足应用工艺的要求。

Abstract: A new anti-mosquito finishing agent has been successfully prepared.Due to its active group and hydrophobic cavity,nonochlorotriazinyl--βcyclodextrin(ab.MCT--βCD) was used to embed DEET which is an anti-mosquito agent.DEET-embedded MCT--βCD was proved by means of ultraviolet-visible detector and the prime technique for preparing DEET-embedded MCT--βCD as an anti-mosquito finishing agent was determined as follows: temperature was 50℃,time was 2 h,stirring velocity was 300 r/min,and the ratio of DEET to MCT--βCD was 2∶1.DEET-embedded MCT--βCD have excellent heat-resistant and alkali-resistant stability,and it can meet the requirement of actual applications.

王树根;徐利.. 一氯均三嗪-β-环糊精包合驱蚊剂的制备[J]. 纺织学报, 2007, 28(10): 70-73.

WANG Shugen;XU Li. Preparation of monochlorotriazinyl-β-cyclodextrin inclusion anti-mosquito complex[J]. JOURNAL OF TEXTILE RESEARCH, 2007, 28(10): 70-73.

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