Journal of Textile Research ›› 2019, Vol. 40 ›› Issue (01): 97-102.doi: 10.13475/j.fzxb.20170203106

• Dyeing and Finishing & Chemicals • Previous Articles     Next Articles

Preparation and microwave absorption property of flexible lightweight magnetic particles-carbon fiber composites

YE Wei1,2, SUN Lei2, YU Jin1,2, SUN Qilong1,2()   

  1. 1. National & Local Joint Engineering Research Center of Technical Fiber Composites for Safety and Protection, Nantong University, Nantong, Jiangsu 226019, China
    2. College of Textiles and Clothing, Nantong University, Nantong, Jiangsu 226019, China
  • Received:2018-02-11 Revised:2018-09-28 Online:2019-01-15 Published:2019-01-18
  • Contact: SUN Qilong E-mail:sunqilong001@ntu.edu.cn

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Abstract:

For developing novel flexible lightweight composite materials having both dielectric loss and magnetic loss abilities, magnetic particles-carbon fiber composites were prepared by impregnating polyacrylonitrile (PAN) based preoxidative fiber felts with metal salt solution and high temperature carbonizing. As-prepared materials were characterized and analyzed by segmental support based adsorption, X-ray diffraction, energy dispersive spectrometry, and scanning electron microscopy. Results show that the prepared composite material was composed of carbon fibers and magnetic Fe-Co-Ni, Fe3O4, Fe-Ni, Fe-Co and so on. The magnetic particles are uniformly distributed along the fiber axis. With the synergistic effects of dielectric loss of magnetic particles and magnetic loss of carbon fibers, such carbon fiber composite materials exhibites excellent microwave absorption property. When the treatment temperature is 650 ℃ and 700 ℃, the absorption bands of electromagnetic wave loss lower than -5 dB are 8.6-18 GHz and 10-18 GHz, respectively, while the absorption frequency are 13.9-18 GHz and 14-18 GHz for those of electromagnetic loss lower than -10 dB. In addtion, the treatment temperature higher than 700 ℃ or lower than 650 ℃ will decrease the adsorption of electromagnetic waves. The microwave absorption property of magnetic particle-carbon fiber composites can controlled by adjusting the treatment temperature.

Key words: composite, carbon fiber, metal salt, magnetic particle, wave absorption property

CLC Number: 

  • TB333

Fig.1

Segmental support wave absorption tester"

Fig.2

XRD patterns of sample"

Fig.3

EDS analysis patterns of fiber surface after hightemperature treatment at 700 ℃."

Fig.4

SEM images and magnetic performance of samples at different treatment temperatures(×500)."

Fig.5

Electromagnetic parameters of samples after different temperature treatments"

Fig.6

Reflection loss curves of different radar frequencies waves. (a) X band; (b) Ku band"

Fig.7

Schemes of electromagnetic loss in composite textile"

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