Journal of Textile Research ›› 2021, Vol. 42 ›› Issue (05): 96-102.doi: 10.13475/j.fzxb.20200707107

• Dyeing and Finishing & Chemicals • Previous Articles     Next Articles

Relationship between Disperse Yellow 6GSL crystal form and thermal stability of its dispersions

WANG Ruifeng1,2, LI Min1,2, TIAN Anli1,2, WANG Chunxia2, FU Shaohai1,2()   

  1. 1. Jiangsu Engineering Research Center for Digital Textile Inkjet Printing, Wuxi, Jiangsu 214122, China
    2. Key Laboratory of Eco-Textiles (Jiangnan University), Ministry of Education, Wuxi, Jiangsu 214122, China
  • Received:2020-07-30 Revised:2021-02-10 Online:2021-05-15 Published:2021-05-20
  • Contact: FU Shaohai E-mail:shaohaifu@hotmail.com

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Abstract:

To address the problem of poor stability of ink-jet printing direct ink under high temperature conditions, this study focused on the relationship between the purification solvent and Disperse Yellow 6GSL crystal form. The effects of grinding process conditions on the particle size and grinding efficiency of the dye dispersion were investigated. The relationship between the crystal form of Disperse Yellow 6GSL and the stability and filtration performance of their dispersions under high temperature conditions was investigated. The results show that the purity of the dye filter cake purified by hot water at 60 ℃ is 99.46%, and the mass ratio of Disperse Yellow 6GSL to home made dispersant 4600W is 1∶1.5. Under the condition that the dispersing machine rotation at 2 500 r/min for initial grinding for 5 h and then grinding for 14 h at a speed of 4 000 r/min, the average particle size of the dye dispersion is 90.39 nm. Before and after the dispersion is conditioned at 60 ℃ for 72 h, the filtration flow rates in the polyvinglidene membrane with an absolute pore size of 1 μm are 428 g/min and 333 g/min. The dispersion have good filtration performance and thermal stability.The dispersions can endow high thermal stability of the disperse dye ink with direct ink-jet printing.

Key words: direct ink-jet printing, dye dispersion, purification, crystal form, thermal stability, ink for direct ink-jet printing

CLC Number: 

  • TS194.2

Fig.1

Effect of purification and dissolution on purity of Disperse Yellow 6GSL"

Fig.2

XRD spectra of Disperse Yellow 6GSL obtained by different purification conditions"

Fig.3

SEM images of Disperse Yellow 6GSL obtained by different purification conditions(×10 000)."

Fig.4

Effect of grinding process conditions on dispersion particle size. (a) Dispersant type; (b) Rotation speed; (c)Solvent agent"

Fig.5

Size distribution curves of dye dispersion"

Fig.6

Relationship between solvent agent and thermal stability of dye dispersion"

Fig.7

Filtration performance of dye dispersion. (a) Filtered membranes of dye dispersions; (b) Filtered membranes after dye dispersions placed at 60 ℃ for 72 h"

Fig.8

Thermal stability of dye dispersion viscosity. (a) Effect of temperature on viscosity; (b) Thermal cycle stability of viscosity"

Fig.9

Zeta potential distribution of dye dispersion"

Fig.10

XRD spectra of dye dispersion purifying by hot water before and after grinding"

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