Journal of Textile Research ›› 2021, Vol. 42 ›› Issue (07): 115-122.doi: 10.13475/j.fzxb.20200907608

• Dyeing and Finishing & Chemicals • Previous Articles     Next Articles

Low-moisture content baking and steaming color fixation process for cotton fabrics padded with reactive dyes

CHEN Xiaowen1,2, WU Wei1,2, ZHONG Yi1,2,3, XU Hong1,2,3, MAO Zhiping1,2,3,4()   

  1. 1. Key Laboratory of Science and Technology of Eco-Textile, Ministry of Education, Donghua University, Shanghai 201620, China
    2. College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, China
    3. Innovation Center for Textile Science and Technology, Donghua University, Shanghai 201620, China
    4. Shanghai ANOKY Group Co., Ltd., Shanghai 201799, China
  • Received:2020-09-29 Revised:2021-01-14 Online:2021-07-15 Published:2021-07-22
  • Contact: MAO Zhiping E-mail:zhpmao@dhu.edu.cn

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Abstract:

To solve the problems of high energy consumption, hydrolysis of reactive dyes, high salinity and high discharge of wastewater in the conventional pad-dry-pad-steam process of cotton fabrics, a low-moisture content baking and steaming color fixation process for cotton fabrics was proposed using a sealed device. The changes of the fabric surface temperature in the sealing device were investigated,and the effects of moisture content on fabric heating and dyeing performance were discussed for theoretical analysis of low-moisture content baking and steaming color fixation for cotton fabrics. To determine the optimal technique, the effects of cotton fabrics baking and steaming temperature and time, and concentrations of substitute alkali and Na2SO4 were explored. Compared with the pad-dry-pad-steam process, the K/S value of the fabric dyed by low-moisture content baking and steaming color fixation process demonstrated an improvement. However, the rubbing fastness of cotton fabrics by the two processes was similar. Incorporating the sealing device in the pad-dye process offers a new method for improving reactive dye properties of cotton fabrics.

Key words: low-moisture content, baking and steaming color fixation, reactive dye, cotton fabric, substitute alkali, pad-dry-pad-steam

CLC Number: 

  • TS193.5

Fig.1

Schematic diagram of sealing device. (a) Exploded view; (b) Side view; (c) Top view"

Fig.2

Temperature change curve of cotton fabric in sealing device"

Fig.3

Temperature change curves of cotton fabric padded with different moisture content in sealing device. (a)Temperature of sealing device 100 ℃;(b) Temperature of sealing device 140 ℃;(c) Temperature of sealing device 170 ℃; (d) Local map within 60 s"

Fig.4

Effect of moisture content on K/S value of dyed fabric and dye fixation rate. (a)Dye concentration 5 g/L; (b) Dye concentration 10 g/L; (c) Dye concentration 30 g/L; (d) Dye concentration 60 g/L"

Fig.5

Effect of temperature on K/S value of dyed fabric and dye fixation rate "

Fig.6

Effect of time on K/S value of dyed fabric and dye fixation rate "

Fig.7

Effect of substituting alkali concentration on K/S value of dyed fabric and dye fixation rate "

Fig.8

Effect of Na2SO4 concentration on K/S value of dyed fabric and dye fixation rate "

Tab.1

K/S value of fabric dyed by different processes "

染料质量浓度/
(g·L-1) 		活性红243染色织物K/S值 活性红198染色织物K/S值 活性红278染色织物K/S值
焙蒸固色
(代用碱) 		焙蒸固色
(混合碱) 		轧烘轧蒸 焙蒸固色
(代用碱) 		焙蒸固色
(混合碱) 		轧烘轧蒸 焙蒸固色
(代用碱) 		焙蒸固色
(混合碱) 		轧烘轧蒸
5 5.82 6.01 3.32 9.44 4.91 2.82 8.75 8.36 6.01
10 9.88 8.68 6.65 14.06 8.75 6.53 13.80 13.06 10.77
20 11.95 11.85 11.49 18.02 15.06 11.98 17.32 16.39 14.59
30 14.43 13.89 12.95 20.38 18.19 14.49 19.81 18.82 16.98
40 15.65 15.27 14.01 21.59 20.41 16.59 20.54 20.07 18.17
50 16.95 16.08 15.94 21.86 21.76 18.03 21.67 20.93 19.31
60 17.90 17.70 16.16 22.19 21.96 18.82 22.21 21.24 20.24

Tab.2

Rubbing fastness of fabric dyed by different processes"

染色
工艺 		染料质量浓度/
(g·L-1) 		耐干摩擦色牢度/级 耐湿摩擦色牢度/级
红243 红198 红278 红243 红198 红278
焙蒸固色
(代用碱) 		10 4~5 5 5 4 4~5 4~5
30 4~5 5 4~5 3 4 4
50 4 4~5 3~4 3 3~4 3~4
焙蒸固色
(混合碱) 		10 5 5 5 4 4~5 4~5
30 5 5 4~5 4 4 3~4
50 5 5 3~4 3~4 3~4 3
轧烘轧蒸 10 5 5 4~5 4~5 4~5 4~5
30 5 5 4 4 4 3~4
50 4~5 5 4 3~4 3~4 3~4
[1] 舒大武. 基于常压饱和蒸汽介质的纤维素织物活性染料湿短蒸染色[D]. 天津: 天津工业大学, 2019: 10-11.
SHU Dawu. Wet short steaming dyeing of cellulose fabric with reactive dyes based on atmospheric pressure saturated steam medium[D]. Tianjin: Tiangong University, 2019: 10-11.
[2] WANG Lili, MA Wei, ZHANG Shufen, et al. Preparation of cationic cotton with two-bath pad-bake process and its application in salt-free dyeing[J]. Carbohydrate Polymers, 2009, 78(3):602-608.
doi: 10.1016/j.carbpol.2009.05.022
[3] 吴春燕. 纺织印染行业常见节能减排措施探讨[J]. 资源节约与环保, 2020(7):9.
WU Chunyan. Discussion on common energy saving and emission reduction measures in textile printing and dyeing industry[J]. Resource Conservation and Environmental Protection, 2020(7):9.
[4] FARIAS L. Progress in chemical foam technology for dyeing applications[J]. AATCC Review, 2013, 13(2):36-41.
[5] MAO Xiaodong, ZHONG Yi, XU Hong, et al. A novel low add-on technology of dyeing cotton fabric with reactive dyestuff[J]. Textile Research Journal, 2018, 88(12):1345-1355.
doi: 10.1177/0040517517700195
[6] ZHANG Xinqing, FANG Kuanjun, ZHANG Jianfei, et al. A vacuum-dehydration aided pad-steam process for improving reactive dyeing of cotton fabric[J]. Journal of Cleaner Production, 2017, 168(12):1193-1200.
doi: 10.1016/j.jclepro.2017.09.112
[7] 李琼, 刘忠延, 刘天强. 烘丝机筒体进出端密封材料选用[J]. 设备管理与维修, 2012(2):54-55.
LI Qiong, LIU Zhongyan, LIU Tianqiang. Selection of sealing material for inlet and outlet of dryer cylinder[J]. Plant Maintenance Engineering, 2012(2):54-55.
[8] 陈林, 王建庆. 活性染料固色率的酸溶解法和尿素剥色法测定[J]. 印染, 2015, 41(1):9-12.
CHEN Lin, WANG Jianqing. Determination of fixation of reactive dyes by acid dissolution method and urea stripping method[J]. China Dyeing & Finishing, 2015, 41(1):9-12.
[9] 王天靖, 臧少玉, 毛志平, 等. ECO型活性染料对棉织物的湿焙连续染色[J]. 纺织学报, 2010, 31(9):62-67.
WANG Tianjing, ZANG Shaoyu, MAO Zhiping, et al. Continuous dyeing of cotton with ECO reactive dyes followed by shortened wet-steaming process[J]. Journal of Textile Research, 2010, 31(9):62-67.
[10] 宋心远. 纤维素纤维纺织品活性染料轧染理论和工艺:二[J]. 印染, 2007(24):42-46,51.
SONG Xinyuan. Theories and processes of pad dyeing of cellulosic textiles with reactive dyestuffs: Ⅱ[J]. China Dyeing & Finishing, 2007(24):42-46,51.
[11] MAO Zhiping, YU Hong, WANG Yuanfeng, et al. States of water and pore size distribution of cotton fibers with different moisture ratios[J]. Industrial & Engineering Chemistry Research, 2014, 53(21):8927-8934.
doi: 10.1021/ie501071h
[12] WANG Huan, KONG Han, ZHENG Jie, et al. Systematically exploring molecular aggregation and its impact on surface tension and viscosity in high concentration solutions[J]. Molecules, 2020, 25(7):1-9.
doi: 10.3390/molecules25010001
[13] GORENEK M. Dye-fibre bond stabilities of some reactive dyes on cotton[J]. Dyes and Pigments, 1999, 40(2):225-233.
doi: 10.1016/S0143-7208(98)00052-7
[14] 张鑫卿, 张健飞, 房宽峻, 等. 应用活性蓝19的棉织物低含水率-湿蒸染色工艺[J]. 纺织学报, 2017, 38(2):129-133.
ZHANG Xinqing, ZHANG Jianfei, FANG Kuanjun, et al. Low-water content wet-steaming fixation of cotton fabric padded with reactive blue 19[J]. Journal of Textile Research, 2017, 38(2):129-133.
[15] 田恬, 冒亚红, 管宇. 安诺素ECO型活性染料对纯棉绒类织物的染色工艺[J]. 纺织学报, 2011, 32(2):79-83.
TIAN Tian, MAO Yahong, GUAN Yu. Dyeing process of Anozol ECO reactive dyes on cotton pile fabrics[J]. Journal of Textile Research, 2011, 32(2):79-83.
[16] 吴伟, 陈小文, 钟毅, 等. 硫酸钠在低带液轧-焙-蒸活性染料染色中的作用[J]. 纺织学报, 2020, 41(5):85-93.
WU Wei, CHEN Xiaowen, ZHONG Yi, et al. Role of sodium sulfate in low add-on pad-cure-steam reactive dyeing process[J]. Journal of Textile Research, 2020, 41(5):85-93.
[17] QI Haisong, CHANG Chunyu, ZHANG Lina. Effects of temperature and molecular weight on dissolution of cellulose in NaOH/urea aqueous solution[J]. Cellulose, 2008, 15(6):779-787.
doi: 10.1007/s10570-008-9230-8
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