纺织学报 ›› 2011, Vol. 32 ›› Issue (3): 15-20.

• 纤维材料 • 上一篇    下一篇

氧化锌纳米纤维的制备及其光催化性能

许淑燕1,2; 张培培1; 熊 杰1

  

  1. 1. 浙江理工大学先进纺织材料与制备技术教育部重点实验室 2. 杭州职业技术学院达利女装学院
  • 收稿日期:2010-03-29 修回日期:2010-06-24 出版日期:2011-03-15 发布日期:2011-03-15
  • 通讯作者: 熊杰

Preparation and photocatalytic properties of ZnO nanofibers

XU Shu-yan1,2; ZHANG Pei-pei1; XIONG Jie1   

  1. 1.The Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Zhejiang Sci-Tech University 2. High Fashion Womenswear Institute, Hangzhou Vacation &Technology College
  • Received:2010-03-29 Revised:2010-06-24 Online:2011-03-15 Published:2011-03-15

摘要:

采用静电纺丝法制备出PVP/Zn(CH3COO)2复合纳米纤维,经烧结得到ZnO纳米纤维。用热重分析仪,X射线能谱仪,傅里叶红外光谱仪,X射线衍射仪和场发射扫描电镜来表征烧结前后纤维的纯度、晶型和表面形貌。以ZnO纳米纤维对亚甲基蓝溶液进行光催化降解研究,考察了光照时间、烧结温度对光催化降解效果的影响。对照自制ZnO纳米颗粒的光催化降解效果,证明ZnO纳米纤维不仅具有良好的光催化性能,还具有很好的重复使用性能。

Abstract:

PVP/Zn(CH3COO)2 composite nanofibers were prepared by electrospinning, and then subjected to high temperature sintering to obtain ZnO nanofibers. Thermal gravimetric analysis, X-ray energy dispersive spectroscopy, fourier transform infrared spectroscopy, X-ray diffraction and field-emission scanning electron microscope were used to characterize the purity, crystal form, and morphology of the fibers before and after sintering. Experiments were carried out using methylene blue(MB) as the pollutant object to evaluate the photocatalytic activity of ZnO nanofibers. The effects of the UV irradiation time and the sintering temperature on the degree of photocatalytic degradation were investigated. Compared to ZnO nanoparticles, it is shown that ZnO nanofibers have good photocatalytic properties and reuse performance.

No related articles found!
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
No Suggested Reading articles found!