Journal of Textile Research ›› 2019, Vol. 40 ›› Issue (04): 83-89.doi: 10.13475/j.fzxb.20171103207

• Dyeing and Finishig & Chemicals • Previous Articles     Next Articles

Ultrasonic treatment of Modal fiber dyed with madder

LI Yang1,2, ZHANG Yuanming2, JIANG Wei1,2, ZHANG Jianming3, WANG Sishe3, SU Jianjun3, HAN Guangting1,2,3()   

  1. 1. College of Textiles & Clothing, Qingdao University, Qingdao, Shandong 266071, China
    2. State Key Laboratory of Bio-Fibers and Eco-Textiles(Qingdao University), Qingdao, Shandong 266071, China
    3. Shandong Hengfeng Plant Dyeing Industrialization Production Technology Research Institute, Dezhou, Shandong 253000, China
  • Received:2017-11-16 Revised:2018-12-17 Online:2019-04-15 Published:2019-04-16
  • Contact: HAN Guangting E-mail:kychgt@qdu.edu.cn

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Abstract:

In order to improve the spinnability of the Modal fiber dyed with madder, ultrasonic treatment was employed to remove the attached particulate matters on the surface of the dyed fibers. The influence of ultrasonic power density, temperature and time on the removal of particulate matters was discussed by single factor test. The experimental factors and levels were selected on the basis of the single factor experiment. The effects of the variates and their interactions on the removal of attached particulate matters on the dyed fiber surface were then studied by the Box-Behnken experiment. The results show that ultrasonic temperature has the greatest effect on the removal of particulate matters on the surface of the fiber, and the influence of power density is the least. The prediction model of regression equation obtained by using Design Expert software has a predictive effect on industrialization. The optimum conditions for the ultrasonic particle removal are as follows: ultrasonic power density of 0.67 W/cm2, ultrasonic temperature of 43 ℃ and ultrasonic time of 22 min.

Key words: plant dyeing, Modal fiber, ultrasonic treatment, Box-Behnken test, madder, dyeing

CLC Number: 

  • TS102.2

Fig.1

Absorption spectrum curve of suspended solids"

Fig.2

Standard curve of suspended solids"

Fig.3

SEM images of Modal fiber before(a) and after(b) dyeing"

Fig.4

Curve of suspended solids' absorbance with time"

Fig.5

Effect of ultrasonic power density on removal of particulate particles on Modal fiber surface"

Fig.6

Effect of ultrasonic temperature on removal of particulate matter on Modal fiber surface"

Fig.7

Effect of ultrasonic action time on removal of particulate matter on fiber surface"

Tab.1

Factor and levels in response surface design"

水平 因素
功率密度/
(W·cm-2)		 超声波处理
时间/min		 超声波处理
温度/℃
-1 0.30 15.0 30
0 0.65 22.5 45
1 1.00 30.0 60

Tab.2

Factor and levels in response surface Box-Behnken design arrangement and corresponding"

序号 编码值 颗粒物质量浓度/(g·L-1)
A B C
1 -1 -1 0 0.114 953
2 1 -1 0 0.152 400
3 -1 1 0 0.124 315
4 1 1 0 0.138 491
5 -1 0 -1 0.132 072
6 1 0 -1 0.169 652
7 -1 0 1 0.179 816
8 1 0 1 0.102 248
9 0 -1 -1 0.163 099
10 0 1 -1 0.112 047
11 0 -1 1 0.113 348
12 0 1 1 0.128 595
13 0 0 0 0.236 254
14 0 0 0 0.222 746
15 0 0 0 0.237 725
16 0 0 0 0.249 761
17 0 0 0 0.225 02

Tab.3

Analysis of variance for each term of fitted regression model"

方差来源 平方和/10-4 自由度 均方/10-3 F值 p值 显著性
模型 400.00 9 4.434 18.600 0.000 4 ***
x1 0.17 1 0.017 0.071 0.797 6
x2 2.04 1 0.204 0.850 0.386 2
x3 3.49 1 0.349 1.470 0.265 3
x1x2 1.35 1 0.135 0.570 0.475 6
x1x3 33.15 1 3.315 13.910 0.007 4 ***
x2x3 10.99 1 1.099 4.160 0.068 9
x12 76.21 1 7.621 31.980 0.000 8 ***
x22 150.00 1 15.000 61.950 0.000 1 ***
x32 88.36 1 8.836 37.080 0.000 5 ***
残差 16.68 7 0.238
失拟相 11.94 3 0.398 3.360 0.136 3
净误差 4.74 4 0.119
总离差 420.00 16

Fig.8

Response surface of ultrasonic power density and time interaction"

Fig.9

Response surface of interaction between ultrasonic power density and temperature"

Fig.10

Response surface of ultrasonic temperature and time interaction"

Fig.11

SEM images of fiber before(a) and after(b) ultrasound treatment(×1 000)"

Fig.12

Comparison of fiber strength before and after ultrasound treatment"

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