分散染料免蒸洗印花糊料的制备及其性能

doi:10.13475/j.fzxb.20210102106

纺织学报 ›› 2022, Vol. 43 ›› Issue (01): 161-166.doi: 10.13475/j.fzxb.20210102106

分散染料免蒸洗印花糊料的制备及其性能

冯冰冰¹^,², 刘艳春¹^,², 周天池³, 白刚¹^,²()

1.绍兴文理学院纺织服装学院, 浙江绍兴 312000
2.浙江省清洁染整技术研究重点实验室, 浙江绍兴 312000
3.盐城工学院纺织服装学院, 江苏盐城 224051

收稿日期:2021-01-11 修回日期:2021-09-10 出版日期:2022-01-15 发布日期:2022-01-28
通讯作者: 白刚
作者简介:冯冰冰(1995—),女,硕士生。主要研究方向为功能纺织品开发。
基金资助:
浙江省基础公益研究计划项目(LCJ18E030002);浙江省基础公益研究计划项目(LCF18E090006)

Preparation and performance of steaming-free and washing-free printing paste with disperse dyes

FENG Bingbing¹^,², LIU Yanchun¹^,², ZHOU Tianchi³, BAI Gang¹^,²()

1. College of Textile and Garment, Shaoxing University, Shaoxing, Zhejiang 312000, China
2. Key Laboratory of Clean Dyeing and Finishing Technology of Zhejiang Province, Shaoxing, Zhejiang 312000, China
3. School of Textile and Apparel, Yancheng Institute of Technology, Yancheng, Jiangsu 224051, China

Received:2021-01-11 Revised:2021-09-10 Published:2022-01-15 Online:2022-01-28
Contact: BAI Gang

摘要/Abstract

摘要：

为解决合成增稠剂在印花过程中对电解质敏感及色浆渗化的问题,通过对合成增稠剂筛选复配,制备出适用于分散染料免蒸洗印花的增稠剂SX-608F。对其黏度、流变性能、染料相容性、抱水性进行测试与表征,并对印花织物的表观得色量、皂洗色牢度和摩擦色牢度进行测试与分析。结果表明:增稠剂SX-608F具有假塑性流体特征,黏度随剪切速率的增加而下降。其印花黏度指数为0.197,触变性良好,黏度回复率为90.40%;在0.1~500 rad/s角频率范围内,储能模量大于损耗模量,损耗系数小于1;与海藻酸钠糊料相比,增稠剂SX-608F印花织物表观得色量高,耐摩擦色牢度和耐皂洗色牢度均可达到4级以上,印制过程无需蒸化和水洗。

关键词: 印花糊料, 免蒸洗, 增稠剂, 抱水性, 流变性, 色牢度

Abstract:

In order to solve the problems of electrolyte sensitivity and color paste infiltration of synthetic thickener in printing process,thickener SX-608F, which is suitable for steaming-free and washing-free printing with disperse dyes, was prepared by screening and compounding. The viscosity, rheological properties, dye compatibility, water holding capacity was analyzed. The apparent color yield, soaping fastness and rubbing fastness of printed fabrics were tested and evaluated. The results showed that thickener SX-608F has the characteristics of pseudoplastic fluid, and the viscosity decreased with the increase of shear rate. The printing viscosity index was 0.197, the thixotropy was good and the viscosity recovery rate was 90.40%. In the frequency range of 0.1~500 rad/s, the storage modulus is larger than the loss modulus, the loss coefficient is less than 1. The printed products of SX-608F thickener have high apparent color yield compared to sodium alginate paste, the soaping fastness and rubbing fastness could reach more than 4 grade. The printing process did not require steaming and washing.

Key words: printing paste, prsteaming-free and washing-free, thickener, water holding capacity, rheology, color fastness

中图分类号:

TS193.62

冯冰冰, 刘艳春, 周天池, 白刚. 分散染料免蒸洗印花糊料的制备及其性能[J]. 纺织学报, 2022, 43(01): 161-166.

FENG Bingbing, LIU Yanchun, ZHOU Tianchi, BAI Gang. Preparation and performance of steaming-free and washing-free printing paste with disperse dyes[J]. Journal of Textile Research, 2022, 43(01): 161-166.

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增稠剂			抱水性/cm		K/S值
种类	质量分数/%		抱水性/cm		K/S值
FL-312		1		0.35		19.24
		2		0.32		21.96
		3		0.10		21.33
		4		0.05		21.06
RG-7202C		1		0.46		14.14
		2		0.45		20.00
		3		0.41		20.86
		4		0.30		21.83
L-101		1		0.78		18.90
		2		0.75		23.34
		3		0.70		23.14
		4		0.50		23.99

防渗化剂质量分数/%	抱水性/cm	K/S值
0	0.30	21.56
1	0.15	22.97
2	0.12	21.82
3	0.10	21.33

质量分数/%	黏度/(Pa·s)		PVI指数
质量分数/%	剪切速率为10 s^-1	剪切速率为100 s^-1	PVI指数
1	1.891	0.551	0.291
2	6.309	1.363	0.216
3	10.990	2.165	0.197
4	16.903	2.997	0.177
5	22.092	3.887	0.176

黏度/(Pa·s)			黏度回复率/%
第1阶段剪切速率1 s^-1	第2阶段剪切速率400 s^-1	第3阶段剪切速率1 s^-1	黏度回复率/%
83.067	0.925	75.803	90.40

染料质量分数/%	抱水性/cm
染料质量分数/%	分散红玉	分散橙	分散深蓝
1	0.01	0.01	0.01
2	0.09	0.10	0.09
3	0.15	0.12	0.14
4	0.20	0.19	0.20
5	0.30	0.25	0.25

分散染料免蒸洗印花糊料的制备及其性能

Preparation and performance of steaming-free and washing-free printing paste with disperse dyes

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参考文献 12

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糊料	处理方式	染料		K/S值				渗透率/%		耐摩擦色牢度/级
糊料	处理方式	染料		正面		反面		渗透率/%		干		湿		涤沾		棉沾	变色
海藻酸钠	还原清洗	分散红玉	16.31		9.61		58.92		5		5		4		4~5		4~5
		分散橙	14.97		6.69		44.69		5		5		5		5		5
		分散深蓝	20.49		8.37		40.85		5		5		4~5		4~5		4
SX-608F	未水洗	分散红玉	20.91		2.21		10.57		4~5		4		4		4~5		4
		分散橙	15.61		1.84		11.79		5		5		5		5		4
		分散深蓝	24.69		1.98		8.02		4~5		4		4~5		4~5		4~5
	还原清洗	分散红玉	20.66		1.82		8.82		5		5		5		5		5
		分散橙	15.02		1.42		9.46		5		5		5		5		5
		分散深蓝	23.77		1.65		6.93		5		5		5		5		5